GE Sievers Innovox Manuals

Manuals and User Guides for GE Sievers Innovox. We have 2 GE Sievers Innovox manuals available for free PDF download: Operation And Maintenance Manual

GE Sievers Innovox Operation And Maintenance Manual (270 pages)

TOC analyzer

Brand: GE | Category: Analytical Instruments | Size: 14.81 MB

Identification Records

3
- Table of Contents
  4
List of Tables

10
List of Figures

11
Revision History

15
Confidentiality

16
Declaration of Conformity

17
Standard Limited Warranty

17
Warnings

20
Chapter 1: Introduction

49
Chapter 2: System Description

51
- System Specifications
  51
  - Additional System Specifications
    53
- Operating Specifications
  53
- Reagent Consumption
  54
- SCWO Method Compliance
  54
- System Overview
  54
  - Figure 1: Analyzer Schematic
    
    56
  - Table 1 Innovox Wetted Materials List
    
    59
  - Additional System Components
    60
    
    System/Controller and Electronics
    60
    
    Clean Water Sample Options
    61
    
    Data Outputs
    61
    
    Sample Preparation Device Options
    61
- Sample Flow Path
  57
Sample Preparation Options

61
Chapter 3: Interferences

67
- Safety
  67
- Reliability
  68
- Analytical Performance
  68
Chapter 4: Installation

71
The Gas-Liquid Separator

79
Analog Outputs (TB1)

81
Stream ID

81
Alarm Outputs (TB3)

82
- Table 5 Binary Input (TB2)
  82
Alarm Outputs (TB4)

83
Figure 8 Wiring Option - Binary Input Using Analyzer's Internal Supply

85
Connecting the Analyzer to a Computer

86
- Installing the USB Connection
  87
Connecting the Analyzer to a Network

87
- Step 7: Connecting to a Power Supply
  88
- Step 8: Connect the Sample Inlet System
  89
  - Installing the Online Sample System
    89
  - Installing the Wastewater Sampler
    90
    
    To Install the Wastewater Sampler (Velocity Method)
    91
Figure 16 Top Wastewater Sampler Bracket W/Plate Adapter

91
Velocity Method - Barb Fittings Identification

92
Figure 19: Velocity Method - Installation

93
Velocity Method - Failsafe Installation

94
Figure 23 Top Wastewater Sampler Bracket W/Plate Adapter

95
Lower Wastewater Sampler Bracket

95
Overflow Method - Failsafe Installation

98
Chapter 5: Calibration and Verification

105
- Overview
  105
- Handling Standards
  106
  - Prepare IC Standard Solution
    106
- Calibration and Verification Options
  107
  - Single-Point Calibration
    107
  - Figure 31 Calibration Curve for Single-Point Calibration
    108
  - Two-Point Calibration
    109
  - Figure 33 Two-Point Calibration (Point 1 Is Reagent Water)
    110
  - Calibration with more than Two Points
    111
    
    Linear Fit Multi-Point Calibration
    111
    
    Point-To-Point Multi-Point Calibration
    112
  - Auto Dilution
    113
  - Blank Correction
    114
  - Calibration Groups
    114
- Table 8 Maximum Dilution Allowed Using Auto Dilution Feature
  
  114
- Preparing for Calibration
  115
  - Save System Settings
    115
  - Perform Maintenance Tasks
    116
- Setting up NPOC, IC, TC/TOC Calibration
  116
- Calibrating the Analyzer
  118
Table 9 Approximate Number of Calibration Repetitions Possible

118
Editing a Calibration

119
Table 10 Approximate Number of Verification Repetitions Possible

122
Chapter 6: Analyzer Operation

123
- Overview
  123
  - The Main Screen
    123
  - Figure 38 the Main Screen (Grab Mode)
    124
- The Menu Screen
  
  125
  - Setting up Measurements (the Setup Tab)
    126
    
    Online Measurements
    126
    
    Continuous Measurements
    127
    
    Cycle Frequency
    128
    
    Operation with Multiple Streams
    128
Figure 43 Operation with Five Streams and the Check Standard

128
Configure Online Screen

129
- Figure 44 Calculating the Run Time
  130
- Online Measurement-Configuration
  131
  - Operation with Multiple Streams
    131
- Figure 46: Stream 1 Screen
  
  132
- Check Standards
  134
Figure 47: Check Standard Setup Screen

135
Check Standard (Setup) Screen

137
- Clean Inlet
  138
- Auto Restart
  138
- Daily Flush
  138
- Summary
  139
- Grab Measurements
  139
  - Figure 51 the Grab (Setup) Screen
    140
  - Table 11 Vial Port - Repetitions Possible
    142
- Rinse
  143
- Measurement Settings
  143
  - Measure
    143
  - Range
    144
  - Auto Range
    144
  - Acid
    145
  - Oxidizer
    145
  - Repetitions
    145
  - Rejects
    145
  - Repeat Criteria
    145
  - Sparge
    146
  - Flush
    146
  - Manual Dilution
    146
  - Configuring Conversion Factors
    146
Figure 52: the Maintenance Tab

147
Configuring the Factor Units

148
- Figure 54: Configuring the Factor Equation
  
  148
- Figure 56: Configuring the Factor Name
  
  149
- User Management
  150
  - Blank Correction
    150
  - Measuring the Blank
    151
The Data Screen

152
- Viewing and Exporting Data
  152
  - Viewing Data on Screen
    152
  - Exporting Data
    152
Export (Data) Screen

153
- Figure 60: Export Data Screen
  
  154
- Reviewing Exported Data
  155
Data Fields Output

155
- Setting up Input and Output (I/O)
  156
  - The I/O Tab
    156
  - Connecting the Analyzer to a Network Via Ethernet
    156
    
    Configuring the Analyzer's IP Address
    156
    
    Configuring a Personal Computer
    157
  - Collecting Historical and Real-Time Data
    159
    
    To Collect Real-Time Data (W/Ethernet Connection)
    159
    
    Configuring Alarm Outputs
    160
    
    Using the Ethernet Connection and Modbus
    160
    
    Figure 62 Alarm Output Screen
    161
    
    Changing the Alarms on or off Setting
    162
    
    Resetting Alarms
    162
  - Printer Setup
    162
  - Liquid Sensor Setup
    163
    
    To Enable a Liquid Sensor
    163
  - Configuring Advanced Setup
    165
    
    Setting Analyzer Name and Location
    165
    
    The Maintenance Tab
    165
    
    Setting System Properties
    166
Figure 65 Liquid Sensor Location - Hazardous Location Enclosure (ATEX or C1/D2)

164
System Properties Screen

166
- Setting the Clock
  167
- Upgrade Option
  167
- Gas Valve PID Parameters
  167
- Cleaning the Analyzer Screen
  168
- Setting the Fail Safe Option
  169
- Setting the Keyboard Options
  169
- Setting the Display Options
  169
- Archiving the Data History
  170
- Shutting down the Analyzer
  170
- Checking the Software Version
  171
Chapter 7: Operation with the Filter Panel

173
- Operation of the Filter Panel with a Sample Pump
  173
- Control of Filter Panel
  173
Figure 69: Blowback Pulses and Sample Flow Time

174
Flush/Blowback Screen

175
Chapter 8: Maintenance

177
- Recommended Spare Parts
  178
- Periodic Maintenance Tasks
  178
  - Periodic Inspections
    178
Consumables Replacement Schedule

178
- Figure 72 Aging of 30% (W/V) Na 2 S 2 O 8 in HDPE Bottles
  
  179
- Preparing the Oxidizer Solution
  179
- Adding the Dilution Water
  180
- Performing a Flush
  180
- Preparing the Acid
  180
- Preparing the Persulfate Oxidizing Solution
  180
  - To Prepare the Oxidizing Solution
    180
- Cleaning the Analyzer
  181
- Cleaning the Gas-Liquid Separator
  181
- Figure 73 the Gas-Liquid Separator
  182
- Cleaning the Sparger
  183
The Sparger

183
- Lubricating the Syringe
  184
Unscrewing the Syringe Base

185
Replacing the NDIR Filter

193
- Replacing the High Pressure Valve Seals
  194
Figure 83: the High Pressure Valve Seal - before Removal

195
The High Pressure Valve Seal - after Removal

195
Table 15 2-Year Maintenance Worksheet - Sievers Innovox Online TOC Analyzer

196
Chapter 9: Troubleshooting

199
- Overview
  199
- Reviewing Warnings and Errors
  199
  - Analyzer Warnings and Error Messages
    200
- Other Software Errors
  
  210
  - Visual Inspection
    210
    
    Figure 85 the Fluidics Side of the Analyzer
    211
    
    Figure 86 the Electronics Side of the Analyzer
    212
    
    Figure 87 Electronics in the Top of the Analyzer
    213
  - Figure 88: Analyzer Schematic
    
    214
  - External Inspection
    215
  - Internal Inspection
    215
  - Reviewing Solutions for Basic Problems
    216
    
    The Analyzer will Not Power on
    216
  - Diagnostics
    217
The Diagnostics Screen

217
- Valves
  218
  - Flow Control Valves
    218
The Flow Control Valve Screen

218
- Figure 93 Sampler Handler Valves Screen
  219
- Gas Valves
  220
Diagnostic Result Screen

220
- Gas Valve Testing Criteria
  221
- Pneumatic Valves
  222
Pneumatic Valve Screen

222
- Heater
  223
  - Heater Testing Criteria
    224
- Ndir
  223
- Liquid Flow Check
  225
- Gas Leak Checks
  226
  - Figure 100 the Gas Leak Check Screen
    227
  - Figure 101 Gas Manifold Leak Check
    229
- Figure 102: Reactor Inlet Valve Leak Check
  
  231
- Figure 103: Reactor Bypass Leak Check
  
  233
- Figure 104 Reactor Leak Check
  235
- Figure 105 Reactor Outlet Valve Check
  237
- Leak Check
  238
- Analog Output
  239
- Binary Output
  239
- Binary Input
  240
- Figure 108 Binary Input Check
  241
- Pumps
  242
- Contacting Technical Support
  243
- Export Diagnostic Data
  243
- Testing the Sparger
  243
- Returning the Analyzer to GE Analytical Instruments
  244
Analyzer Dimensions (Front View)

247
Appendix A: Analyzer Dimension Diagrams

247
Analyzer Dimensions (Right Side View)

248
Analyzer Dimensions (Left Side View)

249
Appendix B: Acronyms and Definitions

251
Appendix C: Importing Analyzer Data into a Spreadsheet

255
- Importing Data into a Spreadsheet Program
  255
  - Figure 114 Microsoft Excel Spreadsheet Screen — Text Import Wizard - Step 1
    256
  - Figure 116 Microsoft Excel Spreadsheet Program — Text Import Wizard - Step 3
    257
Appendix D: Modbus Map

259
Index

265

GE Sievers Innovox Operation And Maintenance Manual (238 pages)

On-Line TOC Analyzer

Brand: GE | Category: Measuring Instruments | Size: 12.08 MB

Identification Records

3
- Table of Contents
  4
List of Tables

10
List of Figures

11
Revision History

14
Confidentiality

15
Declaration of Conformity

16
Standard Limited Warranty

16
Warnings

19
Chapter 1: Introduction

47
Chapter 2: System Description

49
- System Specifications
  49
- System Overview
  52
- Figure 1: Analyzer Schematic
  
  53
- Sample Flow Path
  54
- Additional System Components
  56
  - System/Controller and Electronics
    56
  - Data Outputs
    57
- Major Accessories and Configurations
  57
  - 2-Stream Configuration
    57
  - 5-Stream Configuration
    58
  - Mounting Stand
    58
  - Air Purifier
    58
  - Fail Safe Accessory
    58
  - Ip56
    58
  - NEMA 4X Cabinet
    58
  - Sample Filter Panel
    59
  - Sample Peristaltic Pump
    59
Chapter 3: Interferences

61
- Safety
  61
- Reliability
  62
- Analytical Performance
  62
Chapter 4: Installation

65
The Gas-Liquid Separator

73
- Step 6: Install Input/Output, Cables, and Accessories
  74
- Table 1 Analog Outputs (TB1)
  75
Alarm Outputs (TB3)

76
Table

76
Alarm Outputs (TB4)

77
Figure 8 Wiring Option - Binary Input Using Analyzer's Internal Supply

79
Connecting the Analyzer to a Computer

80
- Installing the USB Connection
  81
Connecting the Analyzer to a Network

81
Chapter 5: Calibration and Verification

89
- Overview
  89
- Handling Standards
  90
  - Prepare IC Standard Solution
    90
- Calibration and Verification Options
  91
  - Single-Point Calibration
    91
  - Two-Point Calibration
    92
Two-Point Calibration (Point 1 Is Standard)

93
Two-Point Calibration (Point 1 Is Reagent Water)

94
Editing a Calibration

105
- Reviewing Calibration and Verification History
  106
Table 7 Approximate Number of Verification Repetitions Possible

106
Chapter 6: Analyzer Operation

107
- Overview
  107
- The Main Screen
  
  108
- The Menu Screen
  
  109
  - Setting up Measurements (the Setup Tab)
    110
    
    Continuous Measurements
    111
    
    Online Measurements
    111
    
    Operation with Multiple Streams
    112
    
    Cycle Frequency
    113
    
    Configuring Online Measurements
    115
  - Figure 25 Operation with Five Streams and the Check Standard
    
    113
  - Figure 26 Calculating the Run Time
    114
Configure Online Screen

115
- Operation with Multiple Streams
  116
Stream 1 Screen

116
- Check Standards
  118
  - Figure 29: Check Standard Setup Screen
    
    119
  - Table 9 Ranges in the Innovox Online TOC Analyzer
    
    128
  - Oxidizer
    129
  - Rejects
    129
  - Repeat Criteria
    129
  - Repetitions
    129
  - Sparge
    129
  - Conversion Factors
    130
  - Flush
    130
  - Manual Dilution
    130
- Check Standard (Setup) Screen
  121
  - Clean Inlet
    122
  - Auto Restart
    122
  - Daily Flush
    122
  - Summary
    123
  - Grab Measurements
    123
  - Table 8 Vial Port - Repetitions Possible
    126
  - Rinse
    127
  - Measurement Settings
    127
    
    Measure
    127
    
    Acid
    128
    
    Auto Range
    128
    
    Range
    128
  - User Management
    131
    
    Blank Correction
    131
    
    Measuring the Blank
    132
The Data Screen

133
- Exporting Data
  134
- Viewing and Exporting Data
  133
  - Viewing Data on Screen
    133
Export (Data) Screen

134
- Figure 36: Export Data Screen
  
  135
- Reviewing Exported Data
  136
Data Fields Output

136
- Setting up Input and Output (I/O)
  137
  - Connecting the Analyzer to a Network Via Ethernet
    137
    
    Configuring the Analyzer's IP Address
    137
    
    Configuring a Personal Computer
    138
    
    Collecting Real-Time Data
    140
    
    Configuring Alarm Outputs
    140
    
    Using the Ethernet Connection and Modbus
    140
    
    Resetting Alarms
    141
  - Printing Data
    141
  - Figure 39 Print Data Screen
    142
  - Configuring Advanced Setup
    143
    
    Setting Analyzer Name and Location
    143
    
    Setting System Properties
    144
  - Setting the Clock
    144
System Properties Screen

144
- Upgrade Option
  145
- Cleaning the Analyzer Screen
  145
- Setting the Fail Safe Option
  145
- Setting the Keyboard Options
  146
- Setting the Display Options
  146
- Archiving the Data History
  146
- Shutting down the Analyzer
  147
Chapter 7: Operation with the Filter Panel

149
- Operation of Filter Panel with Sample Pump
  149
- Control of Filter Panel
  149
Figure 42: Blowback Pulses and Delay

150
Flush/Blowback Screen

151
Consumables Replacement Schedule

153
- Recommended Spare Parts
  154
- Periodic Maintenance Tasks
  154
  - Periodic Inspections
    154
  - Preparing the Oxidizer Solution
    154
Chapter 8: Maintenance

153
- Figure 45 Aging of 30% (W/V) Na
  
  155
- Adding the Dilution Water
  156
- Performing a Flush
  156
- Preparing the Acid
  156
- Cleaning the Analyzer
  157
- Cleaning the Gas-Liquid Separator
  157
The Gas-Liquid Separator

157
- Cleaning the Sparger
  158
The Sparger

158
- Figure 47 the Sparger
  159
- Lubricating the Syringe
  160
  - Figure 49 Unscrewing the Syringe Base
    161
  - Figure 51 Pulling out the Plunger
    162
- Consumables Replacement
  163
- Figure 55: Replacing the NDIR Filter
  
  167
- Entering Consumables Installation Information
  168
- Other Maintenance Tasks
  168
  - Replacing the High Pressure Valve Seals
    168
Figure 56: the High Pressure Valve Seal - before Removal

169
The High Pressure Valve Seal - after Removal

169
Table 12 2-Year Maintenance Worksheet - Sievers Innovox Online TOC Analyzer

170
Chapter 9: Troubleshooting

173
- Overview
  173
- Reviewing Warnings and Errors
  173
  - Analyzer Warnings and Error Messages
    174
- Other Software Errors
  
  182
  - Visual Inspection
    182
    
    Figure 58 the Fluidics Side of the Analyzer
    183
    
    Figure 59 the Electronics Side of the Analyzer
    184
    
    Figure 60 Electronics in the Top of the Analyzer
    185
  - Figure 61: Analyzer Schematic
    
    186
  - External Inspection
    187
  - Internal Inspection
    187
  - Figure 62 Connections to the Gas-Liquid Separator
    188
  - Diagnostics
    189
  - Reviewing Solutions for Basic Problems
    189
    
    The Analyzer will Not Power on
    189
The Diagnostics Screen

189
- Pinch Valves
  190
- Gas Valves
  191
- Ndir
  192
The Temperatures Display on the NDIR Screen

192
- Heater
  193
- Liquid Flow
  194
- Gas Leak Checks
  195
  - Gas Manifold Leak Check
    195
    
    Figure 70: Gas Manifold Leak Check
    197
    
    Figure 71: Reactor Inlet Valve Leak Check
    199
    
    Figure 72: Reactor Bypass Leak Check
    201
    
    Reactor Leak Check
    202
    
    Figure 73: Reactor Leak Check
    203
    
    Reactor Outlet Valve Leak Check
    204
    
    Figure 74 Reactor Valve Outlet Check
    205
    
    Gas Liquid Separator, NDIR Filter, NDIR Sample Path and Sparger Leak Check
    206
  - Reactor Bypass Leak Check
    200
- Reactor Inlet Valve Leak Check
  198
Pneumatic Valve Check

206
- Analog Output
  207
- Binary Output
  207
- Binary Input
  208
- Sample Pumps
  209
- Export Diagnostic Data
  210
- Pneumatic Valves
  206
- Contacting Technical Support
  210
- Returning the Analyzer to GE Analytical Instruments
  210
Analyzer Dimensions (Front View)

213
Appendix A: Analyzer Dimension Diagrams

213
Analyzer Dimensions (Right Side View)

214
Analyzer Dimensions (Left Side View)

215
Appendix B: Acronyms and Definitions

217
Appendix C: Transferring Data to a PC

221
- Using Hyperterminal
  221
  - Figure 84 Entering Connection Information
    222
  - Figure 85 Saving Data on Hyperterminal
    223
- Importing Data into a Spreadsheet Program
  224
  - Figure 87 Microsoft Excel Spreadsheet Screen — Text Import Wizard - Step 1
    225
  - Figure 89 Microsoft Excel Spreadsheet Program — Text Import Wizard - Step 3
    226
Appendix D: Modbus Map

227
Index

233

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GE Sievers Innovox Manuals

GE Sievers Innovox Operation And Maintenance Manual (270 pages)

Table of Contents

Identification Records

List of Tables

List of Figures

Revision History

Confidentiality

Declaration of Conformity

Standard Limited Warranty

Warnings

Chapter 1: Introduction

Chapter 2: System Description

Figure 1: Analyzer Schematic

Table 1 Innovox Wetted Materials List

Sample Preparation Options

Chapter 3: Interferences

Chapter 4: Installation

The Gas-Liquid Separator

Analog Outputs (TB1)

Stream ID

Alarm Outputs (TB3)

Alarm Outputs (TB4)

Figure 9 Wiring Option - Binary Input Using Analyzer's External Supply

Figure 8 Wiring Option - Binary Input Using Analyzer's Internal Supply

Connecting the Analyzer to a Computer

Connecting the Analyzer to a Network

Figure 16 Top Wastewater Sampler Bracket W/Plate Adapter

Velocity Method - Barb Fittings Identification

Figure 17: Lower Wastewater Sampler Bracket

Figure 20 Velocity Method - Adjusting the Sipper Tube Height

Figure 19: Velocity Method - Installation

Velocity Method - Failsafe Installation

Figure 23 Top Wastewater Sampler Bracket W/Plate Adapter

Lower Wastewater Sampler Bracket

Figure 25 Overflow Method - External Sample Pump Position

Figure 26 Overflow Method - Barb Fittings Identification

Figure 28 Overflow Method - Adjusting the Sipper Tube Height

Figure 27: Overflow Method - Installation

Overflow Method - Failsafe Installation

Chapter 5: Calibration and Verification

Table 8 Maximum Dilution Allowed Using Auto Dilution Feature

Table 9 Approximate Number of Calibration Repetitions Possible

Editing a Calibration

Table 10 Approximate Number of Verification Repetitions Possible

Chapter 6: Analyzer Operation

The Menu Screen

Figure 43 Operation with Five Streams and the Check Standard

Configure Online Screen

Figure 46: Stream 1 Screen

Figure 47: Check Standard Setup Screen

Check Standard (Setup) Screen

Figure 52: the Maintenance Tab

Configuring the Factor Units

Figure 54: Configuring the Factor Equation

Figure 56: Configuring the Factor Name

The Data Screen

Export (Data) Screen

Figure 60: Export Data Screen

Data Fields Output

Figure 65 Liquid Sensor Location - Hazardous Location Enclosure (ATEX or C1/D2)

System Properties Screen

Chapter 7: Operation with the Filter Panel

Figure 69: Blowback Pulses and Sample Flow Time

Flush/Blowback Screen

Chapter 8: Maintenance

Consumables Replacement Schedule

Figure 72 Aging of 30% (W/V) Na 2 S 2 O 8 in HDPE Bottles

The Sparger

Unscrewing the Syringe Base

Replacing the NDIR Filter

Figure 83: the High Pressure Valve Seal - before Removal

The High Pressure Valve Seal - after Removal

Table 15 2-Year Maintenance Worksheet - Sievers Innovox Online TOC Analyzer

Chapter 9: Troubleshooting

Other Software Errors

Figure 88: Analyzer Schematic

The Diagnostics Screen

The Flow Control Valve Screen

Diagnostic Result Screen